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Microwave-assisted synthesis, characterization and spectral properties of non-peripherally tetra-substituted phthalocyanines containing eugenol moieties
(Elsevier Science Bv, 2015)
The microwave-assisted synthesis and characterization of novel non-peripherally eugenol substituted metallophthalocyanines (M: Co(II), Ni(II), Cu(II), Zn(II)) have been reported for the first time in this study. All the ...
N-H?N and C-H?? interactions in 4-amino-3-methyl-5-(p- tolyl)-4H-1,2,4-triazole and 4-amino-3-methyl-5-phenyl-4H-1,2,4-triazole
(2006)
The title compounds, C10H12N4, (I), and C9H10N4, (II), have been synthesized and characterized both spectroscopically and structurally. The dihedral angles between the triazole and benzene ring planes are 26.59 (9) and ...
Synthesis and properties of triazol-5-one substituted phthalocyanines by microwave irradiation
(TÜBİTAK, 2006)
Triazol-5-one substituted phthalocyanines were prepared quickly by the reaction of 4-nitrophthalonitrile with anhydrous metal salts in DBU (1,8-diazabicyclo[5,4,0]undec-7-ene) and DMAE (dimethylaminoethanol) by microwave ...
4-Amino-3,5-diethyl-4H-1,2,4-triazole at 100 K: Chains of edge-fused R 44(10) and R44(20) rings
(Wiley, 2007)
The title compound, C6H12N4, has four crystallographically independent mol-ecules in the asymmetric unit. Inter-molecular N - H?N hydrogen bonds involving amino groups and triazole N atoms form a three-dimensional framework ...
2'-[Eth-oxy(p-tol-yl)methyl-ene]acetohydrazide
(2007)
Mol-ecules of the title compound, C12H16N2O2, are linked by N - H?O hydrogen bonds [N?O = 2.971 (2) Å, H?O = 2.17 (2) Å and N - H?O = 162 (2)°] into cyclic centrosymmetric R 2 2(8) dimers. © International Union of ...
2'-[Eth-oxy(phen-yl)methyl-ene]acetohydrazide
(2007)
The title compound, C11H14N2O2, contains two independent mol-ecules in the asymmetric unit. Each independent mol-ecule exists as part of an N - H?O hydrogen-bonded centrosymmetric dimer. © International Union of Crystallography ...
4-(4-Allyl-2-meth-oxyphen-oxy)benzene-1,2-dicarbonitrile
(Wiley, 2007)
In the title compound, C18H14N2O2, the dihedral angle between the two benzene rings is 88.6 (1)°. The allyl group is disordered over two orientations, with refined occupancies of 0.695 (6) and 0.305 (6). The meth-oxy group ...
Synthesis and crystal structure of N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide
(Japan Society for Analytical Chemistry, 2008)
The title compound, N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide, C16H14N4O, crystallizes in the monoclinic space group P21/c with the following unit cell parameters: a = 10.6011(6)Å, b = 7.5676(4)Å, c ...
4-Amino-3-(p-chlorophenyl)-5-(p-methoxybenzyl)-4H-1,2,4-triazole: X-ray and DFT-calculated structures
(2011)
The title compound, 4-amino-3-(p-chlorophenyl)-5-(p-methoxybenzyl)-4H-1,2, 4- triazole I , C16H15ClN4O), has been determined using X-ray diffraction techniques and the molecular structure has also been optimized at the ...