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The microwave-assisted synthesis and characterization of novel polymeric phthalocyanines containing resorcinarene
(0-Belirlenecek, 2008)
Novel metal phthalocyanine (Cu, Zn, Co, Ni) polymers containing resorcinarene moieties were prepared; the resorcinarene was obtained by the acid-catalysed cyclocondensation of resorcinol and acetaldehyde under microwave ...
Synthesis and crystal structure of N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide
(Japan Society for Analytical Chemistry, 2008)
The title compound, N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide, C16H14N4O, crystallizes in the monoclinic space group P21/c with the following unit cell parameters: a = 10.6011(6)Å, b = 7.5676(4)Å, c ...
Microwave-assisted and conventional synthesis of new phthalocyanines containing 4-(p-fluorophenyl)-3-methyl-4,5-dihydro-1H-1,2,4-triazol-5-one moieties
(0-Belirlenecek, 2007)
New metal-free and metal (Zn, Ni, Cu and Co) phthalocyanines containing 4-(p-fluorophenyl)-3-methyl-4,5-dihydro-1H-1,2,4-triazol-5-one moiety have been prepared from 1-(3,4-dicyanophenyl)-4-(p-fluorophenyl)-3-methyl-4,5- ...
2?-[Eth-oxy(p-tol-yl)methyl-ene]acetohydrazide
(0-Belirlenecek, 2007)
Mol-ecules of the title compound, C12H16N2O2, are linked by N - H?O hydrogen bonds [N?O = 2.971 (2) Å, H?O = 2.17 (2) Å and N - H?O = 162 (2)°] into cyclic centrosymmetric R 2 2(8) dimers. © International Union of ...
2?-[Eth-oxy(phen-yl)methyl-ene]acetohydrazide
(0-Belirlenecek, 2007)
The title compound, C11H14N2O2, contains two independent mol-ecules in the asymmetric unit. Each independent mol-ecule exists as part of an N - H?O hydrogen-bonded centrosymmetric dimer. © International Union of Crystallography ...
The microwave-assisted synthesis and characterization of novel, octakis(2-hydroxyethoxy)resorcinarene bridged polymeric metallophthalocyanines
(0-Belirlenecek, 2009)
The new metallophthalocyanine (Zn, Cu, Ni, Co) polymers containing 4,6,10,12,16,18,22,24-octakis(2-hydroxyethoxy)-2,8,14,20-tetramethylresorcinarene are described. Firstly, 4,6,10,12,16,18,22,24-octakis(2-hydroxyethoxy)- ...
Synthesis and properties of triazol-5-one substituted phthalocyanines by microwave irradiation
(0-Belirlenecek, 2006)
Triazol-5-one substituted phthalocyanines were prepared quickly by the reaction of 4-nitrophthalonitrile with anhydrous metal salts in DBU (1,8-diazabicyclo[5,4,0]undec-7-ene) and DMAE (dimethylaminoethanol) by microwave ...
N-H?N and C-H?? interactions in 4-amino-3-methyl-5-(p- tolyl)-4H-1,2,4-triazole and 4-amino-3-methyl-5-phenyl-4H-1,2,4-triazole
(0-Belirlenecek, 2006)
The title compounds, C10H12N4, (I), and C9H10N4, (II), have been synthesized and characterized both spectroscopically and structurally. The dihedral angles between the triazole and benzene ring planes are 26.59 (9) and ...
