dc.contributor.author | Değirmencioğlu, I. | |
dc.contributor.author | Bayrak, R. | |
dc.contributor.author | Er, M. | |
dc.contributor.author | Serbest, K. | |
dc.date.accessioned | 2020-12-19T20:12:08Z | |
dc.date.available | 2020-12-19T20:12:08Z | |
dc.date.issued | 2009 | |
dc.identifier.issn | 0143-7208 | |
dc.identifier.uri | https://doi.org/10.1016/j.dyepig.2009.03.011 | |
dc.identifier.uri | https://hdl.handle.net/11436/3839 | |
dc.description.abstract | Novel polymeric metal-free and metallo(Cu(II), Co(II), Ni(II), Zn(II) and Pb(II))-phthalocyanine complexes were synthesized using microwave irradiation and the products were purified by several (crystallization and preparative thin layer) techniques. The newly prepared compounds were characterized by a combination of elemental analyses, IR, 1H/13C NMR, 1H-1H COSY, MS and UV-Vis spectroscopy. In order to better understand the spectroscopy data (especially for 1H/13C NMR and 1H-1H COSY techniques), computational calculations were used for characterization at DFT/6-31G(d) level. The electronic spectra exhibited an intense ? ? ?* transition with characteristic Q and B bands of the phthalocyanine core. © 2009 Elsevier Ltd. All rights reserved. | en_US |
dc.description.sponsorship | Karadeniz Teknik Üniversitesi: 2006.111.002.4 | en_US |
dc.description.sponsorship | This work was supported by the Research Fund of Karadeniz Technical University, Project No. 2006.111.002.4 (Trabzon/Turkey). | en_US |
dc.language.iso | eng | en_US |
dc.publisher | 0-Belirlenecek | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Microwave-assisted | en_US |
dc.subject | Phthalodinitrile | en_US |
dc.subject | Polymeric phthalocyanines | en_US |
dc.subject | Spectroscopic identification | en_US |
dc.subject | Substituted Schiff base | en_US |
dc.subject | Synthesis | en_US |
dc.title | The microwave-assisted synthesis and structural characterization of novel, dithia-bridged polymeric phthalocyanines containing a substituted thiophenylamine Schiff base | en_US |
dc.type | article | en_US |
dc.contributor.department | RTEÜ | en_US |
dc.identifier.doi | 10.1016/j.dyepig.2009.03.011 | |
dc.identifier.volume | 83 | en_US |
dc.identifier.issue | 1 | en_US |
dc.identifier.startpage | 51 | en_US |
dc.identifier.endpage | 58 | en_US |
dc.relation.journal | Dyes and Pigments | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |