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Microwave-assisted synthesis and biological evaluation of some coumarin hydrazides

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info:eu-repo/semantics/openAccess

Date

2018

Author

Yılmaz, Fatih
Faiz, Özlem

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Citation

Yılmaz, F. & Faiz, Ö. (2018). Microwave-assisted synthesis and biological evaluation of some coumarin hydrazides. Journal of the Turkish Chemical Society, Section A: Chemistry, 5(2), 551-568. https://doi.org/10.18596/jotcsa.390928

Abstract

In this work, 15 different coumarin hydrazides were successfully synthesized and screened for their antioxidant and antilipase activities. To do this, firstly, salicylaldehyde derivatives and Meldrum's Acid were reacted in absolute ethanol with catalytic amount of pyridine to obtain coumarin-3-carboxylic acid derivatives (1a-e). Then, these compounds were treated with 1H-benzotriazole in dichloromethane by using thionyl chloride to synthesize benzotriazole derivatives (2a-e). Then, compounds 2a-e were reacted with three commercial hydrazides (nicotinic hydrazide, benzhydrazide,and phenyl acetichydrazide) in ethanol by using microwave irradiation and conventional heating procedures to obtain final products (3-5a-e). Finally, these compounds were tested for their anti-oxidant and anti-lipase activities. The structure of newly synthesized compounds was identified by IR, 1H NMR, 13C NMR, and elemental analysis data.

Source

Journal of the Turkish Chemical Society, Section A: Chemistry

Volume

5

Issue

2

URI

https://doi.org/10.18596/jotcsa.390928
https://app.trdizin.gov.tr/makale/TXpJMU1ERXlNZz09
https://hdl.handle.net/11436/5585

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  • FEF, Kimya Bölümü Koleksiyonu [477]
  • Scopus İndeksli Yayınlar Koleksiyonu [6023]
  • Teknik Bilimler Meslek Yüksekokulu Koleksiyonu [201]
  • TR-Dizin İndeksli Yayınlar Koleksiyonu [2844]

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