Yayın tarihi için FEF, Kimya Bölümü Koleksiyonu listeleme
Toplam kayıt 437, listelenen: 101-120
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Synthesis and in vitro antioxidant activities of novel 4-(3-methyl-2- thienylmethyleneamino)-4,5-dihydro-1H-1,2,4-triazol-5-one derivatives with their acidic properties
(2013)In the present study 3-alkyl(aryl)-4-amino-4,5-dihydro-1H-1,2,4-triazol-5- ones 2a-i reacted with 3-methyl-thiophene-2-carboxyaldehyde to afford the corresponding 3-alkyl(aryl)-4-(3- methyl-2-thienylmethyleneamino)-4,5-dihydro- ... -
Water-soluble phthalocyanines containing azo dye; microwave-assisted synthesis and photochemical properties of ZnPcs
(Bilimsel Teknik Araştırma Konseyi Türkiye- TÜBİTAK, 2014)Novel water-soluble metallophthalocyanines (M: Co, Ni, Cu, Zn) containing azo dye were characterized. The structures were confirmed by IR, UV/vis, 1 H NMR, 13C NMR, mass spectroscopy, and elemental analysis. Photochemical ... -
4-Methyl-N-(4-methylphenylsulfonyl)-N-phenylbenzenesulfonamide
(Int Union Crystallography, 2014)The whole molecule of the title compound, C20H 19NO4S2, is generated by twofold rotational symmetry. The N atom is located on the twofold rotation axis and has a trigonal-planar geometry. It is bonded by two S atoms of two ... -
Chemical composition and antimicrobial activity of essential oils from tortella inclinata var. Densa, T. Tortusa and pleurochaete squarrosa
(Chemical Publishing Co., 2014)Although some chemical compositional data are available about the extracts of Tortella tortusa and Pleurochaete squarrosa, there is no investigation about the compositions and antimicrobial activities of the volatiles from ... -
Essential oil analysis and antimicrobial activity of neckera complanata (Hedw.) huebener and neckera crispa Hedw. (Neckeraceae) grown in Turkey
(Chemical Publishing Co., 2014)In this work, the essential oils obtained by hydrodistillation from Neckera complanata (Hedw.) Huebener and Neckera crispa Hedw (Neckeraceae) were analyzed by GC-FID and GC-MS. Twenty-one compounds in the oil of N. complanata, ... -
Microwave-assisted synthesis of some hybrid molecules containing penicillanic acid or cephalosporanic acid moieties and investigation of their biological activities
(Springer Birkhauser, 2014)Ethyl 4-amino-2-fluorophenylpiperazin-1-carboxylates containing a 1,3-oxazol(idin)e, 5-thioxo-1,2,4-triazole, 1,3,4-thiadiazole, 5-thioxo-1,3,4-oxadiazole, or 1,3-thiazole nucleus were obtained starting from ethyl ... -
Microwave-assisted synthesis of new benzimidazole derivatives with lipase inhibition activity
(Taylor & Francis Ltd, 2014)A practical protocol has been used for the synthesis of benzimidazoles. the reaction of iminoester hydrochlorides of phenylacetic with 4,5-dichloro-1,2-phenylenediamine under microwave irradiation leads to the benzimidazole ... -
Cholesterol forms and traditional lipid profile for projection of atherogenic dyslipidemia: lipoprotein subfractions and erythrocyte membrane cholesterol
(Springer, 2014)Atherogenic dyslipidemia characterized by abnormal changes in plasma lipid profile such as low high-density lipoprotein (HDL) and increased triglyceride (TG) levels is strongly associated with atherosclerotic diseases. We ... -
Synthesis and pharmacological activities of some new 2-[1-Heptyl-3-(4-methoxybenzyl)-5-oxo-1,5-dihydro-4H-1,2,4-triazol-4-yl] acetohydrazide derivatives
(Walter de Gruyter Gmbh, 2014)In the present investigation, the key intermediate acetohydrazide derivative 5 was synthesized starting from 3-(4-methoxybenzyl)-4-amino-4,5-dihydro-1,2,4-triazol-5-one (1) by a four-step reaction. Thiosemicarbazides 6a-f ... -
Synthesis, aggregation and spectroscopic studies of novel water soluble metal free, zinc, copper and magnesium phthalocyanines and investigation of their anti-bacterial properties
(Pergamon-Elsevier Science Ltd, 2014)In this study, novel phthalonitrile derivative (3) was synthesized by the reaction between 4-nitrophthalonitrile (2) and a triazole derivative (1) containing pyridine moiety. Crystal structure of compound (3) was characterized ... -
Synthesis of some new 1,2,4-triazole derivatives starting from 3-(4-chlorophenyl)-5-(4-methoxybenzyl)-4H-1,2,4-triazol with anti-lipase and anti-urease activities
(Wiley-V C H Verlag Gmbh, 2014)In the present study, starting compound 4 was prepared by deamination of compound 2 in the presence of hypophosphorous acid and sodium nitrite. Treatment of compound 4 with ethyl bromoacetate produced ethyl[3-(4-chloroph ... -
Rapid synthesis and lipase inhibition activity of some new benzimidazole and perimidine derivatives
(Maik Nauka/Interperiodica/Springer, 2014)This study presents a synthesis of new series of some benzimidazole, bisbenzimidazole and perimidine derivatives via microwave technique, which, leads to the good product yields and short reaction times. the structure of ... -
Microwave-assisted preparation of azachalcones and their N-alkyl derivatives with antimicrobial activities
(Taylor & Francis Ltd, 2014)Two new azachalcones were prepared by both Claisen-Schmidt condensation and a simple environmentally trendy microwave-assisted method. Ten new N-alkyl (C-6,C-8,C-10,C-12,C-14)-substituted azachalconium bromides (3a-e, 4a-e) ... -
Microwave-assisted synthesis of some 2-substituted quinazolin-4(3h)-one derivatives from imıioester hydrochlorides
(Editura Acad Romane, 2014)Herein, a method that involves a reaction of iminoester hydrochloride with methyl anthranilate via microwave assisted synthesis is reported. This efficient procedure provides pure products within few minutes. This method ... -
Synthesis, spectroscopic and structural studies of 4-Amino-3-(ethyl)-5-(4-chlorophenyl)-4H-1,2,4-triazole and 4-Amino-3-cyclopropyl-5-oxo-4,5-dihydro-1,2,4-triazole-1-yl-acetic acid ethyl ester
(Elsevier Science Bv, 2014)The title compounds of 4-Amino-3-(ethyl)-5-(4-chlorophenyl)-4H-1,2,4-triazole (I, C10H11ClN4) and 4-Amino-3-cyclopropyl-5-oxo-4,5-dihydro-1,2,4-triazol-1-yl-acetic acid ethyl ester (II, C9H14N4O3), have been determined ... -
Pyronin Y (basic xanthene dye)-bentonite composite: a spectroscopic study
(Elsevier Science Bv, 2014)The expansion by 1.43 Angstrom of basal spacing and the shift to higher frequencies of in-plane ring vibrations of the Pyronin Y molecule at 1603 and 1527 cm(-1) on the formation of Pyronin Y-bentonite composite exhibited ... -
Computational studies on the anastrozole and letrozole, effective chemotherapy drugs against breast cancer
(Pergamon-Elsevier Science Ltd, 2014)In this paper, computational studies were carried out on anastrozole and letrozole, chemotherapy drugs used against breast cancer. Optimization and frequency calculations were performed at B3LYP/6-31G (d) basis set and ... -
Determination of hydroquinone using Poly(3-methylthiophene) hynthesized electrochemically on Pt electrode in methylene chloride
(Wiley-Blackwell, 2014)Poly(3-methylthiophene) (P3MT) film was synthesized by potentiodynamic method on Pt electrode in methylene chloride solution containing 0.10M tetrabuthlammonium perchlorate supporting electrolyte and used for the determination ... -
Microwave-assisted synthesis of some novel benzimidazole derivatives containing imine function and evaluation of their antimicrobial activity
(Wiley, 2014)4-Bromo-o-phenylenediamine and ethylimido-p-bromophenylacetate, 1, were subjected to microwave irradiation to synthesize benzimidazole derivative, compound 2. Ester derivative, 3, and hydrazide derivative, 4, of compound ... -
Synthesis of some novel 1,2,4-triazol-3-one derivatives bearing the salicyl moiety and their anticonvulsant activities
(Wiley-V C H Verlag Gmbh, 2014)A series of new 1,2,4-triazole-3-one derivatives bearing the salicyl moiety were synthesized by using microwave irradiation, and their chemical structures were identified by IR, H-1 NMR, C-13 NMR, elemental analysis, and ...