Yayın tarihi için FEF, Kimya Bölümü Koleksiyonu listeleme
Toplam kayıt 425, listelenen: 61-80
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Experimental and theoretical study on the structure and vibrational spectra of β-2-aminopyridinium dihydrogenphosphate
(Elsevier, 2011)Experimental and theoretical vibrational spectra of ?-2- aminopyridinium dihydrogenphosphate (?-2APDP) have been investigated. The FT-IR spectrum of ?-2APDP was recorded in the region 4000-400 cm -1. The optimized molecular ... -
Structural analysis of naproxen-intercalated bentonite (Unye)
(Elsevier, 2011)The difference in the basal spacing (8.79Å) and a higher mass loss (6.2%) in the temperature range of 200-750°C of naproxen-bentonite (N-bentonite) comparing to that of Unye bentonite (UB) signified the existence of thermally ... -
Silorane-based composite: Depth of cure, surface hardness, degree of conversion, and cervical microleakage in class II cavities
(Wiley, 2011)Objective: The purpose of this study was to determine the depth of cure, degree of conversion (DC), hardness, and cervical sealing ability of silorane-based composite (Filtek Silorane [FS; 3M, Seefeld, Germany]) and to ... -
Determination of the pKa of Some triazole derivatives by the potentiometric method in dioxan-water mixtures
(2011)Stoichiometric protonation constants of some 3-alkyl(aryl)-4-(substituted benzylamino)-4,5-dihydro-1 H-1,2,4-triazol-5-ones derivatives were determined potentiometrically in 50% (v/v) dioxan-water mixtures at 25°C with an ... -
Synthesis of novel triazol compounds containing isatin as potential antibacterial and antifungal agents by microwave and conventional methods
(Sage Publishing, 2011)Microwave irradiation has been used to accelerate the conversion of isatin (1a) and 5-nitroisatin (1b) into their Schiff bases 3-[5?-aryl(alkyl)- 2?,4?-dihydro-1?,2?,4?-triazol-3?-on- 4?-yl]iminoisatin (3a-g) and ... -
New olefinic centred binuclear clamshell type phthalocyanines: Design, synthesis, structural characterisation, the stability and the change in the electron cloud at olefine-based symmetrical diphthalonitrile fragment by the combined application of UV-Vis electronic structure and theoretical methods
(Elsevier, 2011)The olefinic centred Schiff base (3) was obtained from the condensation of substituted dialdehyde (1) with 2-amino-4-methylphenol (2) in a 1:2 ratio. The diphthalonitrile derivative (5) was prepared by the reaction of ... -
Determination of protonation constants of some 3-alkyl(aryl)-4-(ptert- butyl(benzyl/benzyliden)amino)-4,5-dihydro-1H-1,2,4-triazole-5- one deriveatives with spectrophotometric method
(2011)The protonation constant values of different twelve 3-alkyl(aryl)-4-(p-t-butyl(benzyl/ benzyliden)amino)-4,5-dihydro-1H-1,2,4-triazole-5-one derivatives have been determined in ethanol %50 - water %50 mixtures by ... -
4-Amino-3-(p-chlorophenyl)-5-(p-methoxybenzyl)-4H-1,2,4-triazole: X-ray and DFT-calculated structures
(2011)The title compound, 4-amino-3-(p-chlorophenyl)-5-(p-methoxybenzyl)-4H-1,2, 4- triazole I , C16H15ClN4O), has been determined using X-ray diffraction techniques and the molecular structure has also been optimized at the ... -
Structural characterization of aniline-bentonite composite by FTIR, DTA/TG, and PXRD analyses and BET measurement
(Taylor & Francis, 2011)The aniline species incorporated into the acid-activated bentonite matrices leads to the decay of the skeletal stretches centered at 1041 cm-1 and the rise of new features in the phenyl ring frequency region, 1700-1400 ... -
Novel coordination polymers of metal(II) succinates with 4-aminopyridine: Synthesis, spectroscopic, thermal, and fluorescent properties
(Wiley, 2011)Four novel divalent transitional metal succinates (suc) with 4-aminopyridine (apy), [M(apy)2(H2O)2(?-suc) ]n [M = Ni (1), Co (2)] and [M(apy)2(H2O)(suc)] [M = Cu (3), Zn (4)] were synthesized and characterized by elemental ... -
Syntheses, crystal structures, fluorescent, and thermal properties of nickel(II) 5,5-diethylbarbiturate complexes with (2-aminomethyl), (2-aminoethyl), and (2-hydroxyethyl)pyridines
(Taylor & Francis, 2011)Three nickel(II) complexes of 5,5-diethlybarbiturate (barb) with (2-aminomethyl)pyridine (ampy), (2-aminoethyl)pyridine (aepy), and (2-hydroxyethyl)pyridine (hepy), [Ni(barb-N)2(ampy)2] (1), [Ni(barb-N,O)(aepy)2](barb)·H2O ... -
InVitro antioxidant activities of new 4,5-dihydro-1H-1,2,4-triazol-5-ones having thiophene ring with their acidic properties
(Hindawi, 2011)Seven new 3-alkyl(aryl)-4-(2-thienymethylenamino)-4,5-dihydro- 1H-1,2,4-triazol-5-ones (2) were synthesized by the reactions of 3-alkyl(aryl)- 4-amino-4,5-dihydro-1H-1,2,4-triazol-5-ones (1) with thiophene-2-carbaldehyde. ... -
Effect of microwave irradiation on the synthesis of 1,2,4-triazol-3-one derivatives and their antimicrobial activities
(Science Reviews 2000 Ltd, 2012)An easy efficient method for the synthesis of N-(3,5-dichlorophenyl)-5-alkyl/aryl-3H-1,2,4-triazol-3-one derivatives under microwave irradiation has been developed using the reaction of 3,5-dichloroaniline and ethoxycarb ... -
Synthesis, characterization, spectral and electrical properties of peripherally tetratriazole-substituted phthalocyanines and its metal complexes
(Elsevier, 2012)The substituted [1,2,4]triazole 3 was obtained from the reaction between compound 1 and compound 2. Novel substituted phthalonitrile 5 was prepared by the substitution of the nitro group of 4-nitrophthalonitrile 4 with ... -
Poly(vinylferrocenium) perchlorate-polyaniline composite film-coated electrode for amperometric determination of hydroquinone
(Springer, 2012)Poly(vinylferrocenium) perchlorate-polyaniline (PVF +-PANI) composite film was synthesized electrochemically on Pt electrode in a methylene chloride solution containing a mixture of poly(vinylferrocene) (PVF) polymer and ... -
Microwave-assisted synthesis of some new benzylidenamino compounds and potentiometric determination of their pKa
(2012)A growing body of literature has shown the effectiveness of using microwaves in chemical reactions. The aim of this study is to demonstrate a rapid and highly efficient synthesis of some new benzylidenamino compounds (4a-f) ... -
Composition and antimicrobial activity of essential oil from the flower of Rhododendron luteum Sweet
(Chemical Publishing Co., 2012)Essential oil from air-dried flower of Rhododendron luteum Sweet (Ericaceae), was obtained by hydrodistillation in a Clevenger-type apparatus and analyzed by GC-MS and GC-FID. Sixty-four components were identified in the ... -
Solvothermal synthesis and characterization of coordination polymers of cobalt(II) and zinc(II) with succinic acid
(Springer, 2012)The complexes [Co(C 4H 4O 4)] n (1) and [Zn(im)2- (C 4H 4O 4)] n (2) (C 4H 4O 4 = succinate dianion, suc; im = imidazole) have been synthesized solvothermally and characterized by elemental analysis, IR, TG-DTA, and ... -
In vitro antioxidant and acidic properties of novel 4-(5-Methyl- 24hienylmethyleneamino)-4,5-dihydro-1H-l,2,4-triazol-5one derivatives. Synthesis and characterization
(Syscom 18 SRL, 2012)In the present study 3-alkyl(aryl)-4-amino-4,5-dihydro-1H-l,2,4-triazol-5- ones 2a-i reacted with 5-methylthiophene-2-carboxyaldehyde to afford the corresponding compounds 3a-i and the acetylation reactions of compounds ... -
Efficient microwave assisted synthesis of some new benzimidazoles containing the mebendazole nucleus
(Science Reviews 2000 Ltd, 2013)A simple and practical method has been developed for the synthesis of benzimidazoles containing the biological active mebendazole nucleus. Iminoester hydrochlorides of phenylacetic acids were used as intermediates in the ...