Yayın tarihi için FEF, Kimya Bölümü Koleksiyonu listeleme
Toplam kayıt 410, listelenen: 21-40
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Synthesis and anticancer evaluation of some new 4-amino-3-(p-methoxybenzyl) -4,5-dihydro-1,2,4-triazole-5-one derivatives
(Verlag der Zeitschrift fur Naturforschung, 2008)4-Amino-3-p-methoxybenzyl-5-oxo-4,5-dihydro-1,2,4-triazol-1-yl-acetic acid ethyl ester (2) was prepared from 4-amino-4,5-dihydro-1H-1,2,4-triazole-5-one (1) and ethyl bromoacetate. Compound 3 was synthesized by the ... -
Synthesis, potentiometric titrations and antioxidant activities of some 4-acylamino-4,5-dihydro-1H-1,2,4-triazol-5-one derivatives
(2008)Five novel 3-alkyl-4-cinnamoylamino-4,5-dihydro-1H-1,2,4-triazol-5-ones (2) were synthesized by the reactions of 3-alkyl-4-amino-4,5-dihydro-1H-1,2,4- triazol-5-ones (1) with cinnamoyl chloride and characterized by elemental ... -
The microwave-assisted synthesis and characterization of novel polymeric phthalocyanines containing resorcinarene
(Elsevier, 2008)Novel metal phthalocyanine (Cu, Zn, Co, Ni) polymers containing resorcinarene moieties were prepared; the resorcinarene was obtained by the acid-catalysed cyclocondensation of resorcinol and acetaldehyde under microwave ... -
Synthesis and crystal structure of N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide
(Japan Society for Analytical Chemistry, 2008)The title compound, N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide, C16H14N4O, crystallizes in the monoclinic space group P21/c with the following unit cell parameters: a = 10.6011(6)Å, b = 7.5676(4)Å, c ... -
Studies on the protonation constants of some triazoles in ethanol-water mixtures
(Chemical Publishing Co., 2008)Several studies, involving the formation and investigation of biological activities of some triazoles derivatives. These derivatives have weak acidic properties. To gain more information about the effect of solvent on ... -
Reversible immobilization of catalase by using a novel bentonite-cysteine (Bent-Cys) microcomposite affinity sorbents
(Elsevier, 2008)This study focused on developing bentonite-cysteine (Bent-Cys) microcomposite affinity sorbents (38-105 ?m) for catalase adsorption from aqueous solutions. Pseudo-biospecific affinity ligand l-cysteine was covalently binded ... -
Determination of the protonation constants of triazole derivatives in non-aqueous solvents
(2009)Different 17 triazole derivatives were titrated with tetrabutylammonium hydroxide in four non-aqueous solvents (isopropyl alcohol, rert-butyl alcohol, N,N-dimethylformamide and acetonitrile), using Potentiometric method. ... -
Structural analysis of reactive dye species retained by the basic alumina surface
(Springer, 2009)The alumina-dye composites were prepared by treating the basic alumina with the water solutions of Reactive Red 120 (RR 120) and Reactive Blue 15 (RB 15) dyes. The bands of low intensities in the 1400-1600 cm-1 region and ... -
The microwave-assisted synthesis and characterization of novel, octakis(2-hydroxyethoxy)resorcinarene bridged polymeric metallophthalocyanines
(Elsevier, 2009)The new metallophthalocyanine (Zn, Cu, Ni, Co) polymers containing 4,6,10,12,16,18,22,24-octakis(2-hydroxyethoxy)-2,8,14,20-tetramethylresorcinarene are described. Firstly, 4,6,10,12,16,18,22,24-octakis(2-hydroxyethoxy)- ... -
Synthesis of methyl (E)-2′,4″-thiazachalcones and their N-alkyl derivatives, photochemistry with theoretical calculations and antimicrobial activities
(TUBİTAK, 2009)A series of 9 new (E) -thiazachalcones (1-3), and their N -alkyl substituted derivatives (4-6), and stereoselective dimerization products (7-9) were synthesized, then tested for antimicrobial activity against all test ... -
Synthesis of 1,2,4-Triazole derivatives and determination of protonation constant
(2009)A microwave irradiation method has been developed for the synhesis of some 1,2,4-triazole derivatives using environmentally benign solvent ethanol in open vessels. Twelve 1,2,4-triazole derivatives were synthesized in good ... -
Determination of adsorptive properties of a Turkish Sepiolite for removal of Reactive Blue 15 anionic dye from aqueous solutions
(Elsevier, 2009)Reactive Blue 15 (RB 15) adsorption on the Turkish Sepiolite was carried out by batch equilibrium technique. IR spectrum and surface area measurement of the composite of dye-sepiolite (Turkish) pointed out that dye species ... -
3-Ethyl-4-(p-chlorobenzylidenamino-4,5-dihydro-1H-1,2,4-triazol-5-one (EPHBAT) as precipitant for carrier element free coprecipitation and speciation of chromium(III) and chromium(VI)
(Elsevier, 2009)A method for the separation and speciative determination of Cr(VI) and Cr(III) has been developed. The procedure is based on coprecipitation of Cr(III) on 3-ethyl-4-(p-chlorobenzylidenamino-4,5-dihydro-1H-1,2,4-triazol-5-one ... -
Performance of magnesium oxide-coated bentonite in removal process of copper ions from aqueous solution
(Elsevier, 2010)This paper presents the adsorption of Cu(II) ions from aqueous solution on modified Unye bentonite. Adsorption of Cu(II) ions by magnesium oxide-coated bentonite (MCB) sample was investigated as a function of the initial ... -
Equilibrium and kinetic studies on the removal of basic dye using raw and thermal-activated fatsa bentonite
(2010)The adsorption behavior of crystal violet (CV+) from aqueous solution onto raw Fatsa (RFB) and thermalactivated Fatsa (TAFB) bentonite samples was investigated as a function of parameters, such as pH, temperature, initial ... -
Novel phthalocyanines containing substituted salicyclic hydrazone-1,3-thiazole moieties: Microwave-assisted synthesis, spectroscopic characterization, X-ray structure and thermal characterization
(Elsevier, 2010)Novel, metal-free and metallo(Cu, Co, Ni, Zn, Pb and Mn)phthalocyanine compounds were synthesized by exposure to microwave irradiation and the products purified. The newly prepared compounds were characterized using elemental ... -
Purification and characterisation of a polyphenol oxidase from Boletus erythropus and investigation of its catalytic efficiency in selected organic solvents
(Elsevier, 2010)Polyphenol oxidase (PPO) was purified from Boletus erythropus using a Sepharose 4B-L-tyrosine-p-amino benzoic acid affinity column. Optimum pH and temperature were found to be 8.0 and 20 °C, respectively, using 4-methylcatechol ... -
Metal(II) nicotinamide complexes containing succinato, succinate and succinic acid: Synthesis, crystal structures, magnetic, thermal, antimicrobial and fluorescent properties
(Springer Link, 2010)Four novel divalent transitional metal succinates (suc) with nicotinamide (nia), {[M(?-suc)(H 2O) 2(nia) 2]·2H 2O} n [M = Mn (1), Ni (2)], [Cu(suc)(nia) 2] (3) and [Ni(H 2O) 4(nia) 2](suc)·(H 2suc) (4), have been synthesized ... -
The spectral, structral and thermal characterizations of dimethyl sulphoxide, pyridine, ethanolamine and N-methyl formamide intercalated kaolinites
(Verlag der Zeitschrift fur Naturforschung, 2010)The intercalation of dimethyl sulphoxide (DMSO), pyridine (Py), ethanolamine (Ea), and Nmethyl formamide (NMF) molecules into the kaolinite interlayers led to an appreciable decrease of 3697 cm-1 of the hydroxyl band. The ... -
Cloning, expression and characterization of highly thermo- and pH-stable maltogenic amylase from a thermophilic bacterium Geobacillus caldoxylosilyticus TK4
(Elsevier, 2010)Maltogenic amylases (MAases), a subclass of cyclodextrin (CD)-hydrolyzing enzymes, belong to glycoside hydrolase family 13. A gene corresponding to MA in Geobacillus caldoxylosilyticus TK4 (GcaTK4MA) was cloned into pET28a(+) ...
